The Effect of Temperature and Extraction Time of Cinnamon (Cinnamomum burmannii) on Physicochemical and Organoleptic Properties of Herbal Paper Soap

Authors

  • N Narsih Department of Agricultural Technology, Politeknik Negeri Pontianak, Pontianak, Indonesia
  • Y. Erning Indrastuti Department of Agricultural Technology, Politeknik Negeri Pontianak, Pontianak, Indonesia
  • S Saniah Department of Agricultural Technology, Politeknik Negeri Pontianak, Pontianak, Indonesia
  • Borneo Satria Pratama Department of Agricultural Technology, Politeknik Negeri Pontianak, Pontianak, Indonesia
  • Desi Ramayanti Department of Agricultural Technology, Politeknik Negeri Pontianak, Pontianak, Indonesia

DOI:

https://doi.org/10.58905/demeter.v2i2.404

Abstract

This study aims to examine the effects of cinnamon (Cinnamomum burmannii) extraction temperature and duration on the physicochemical and organoleptic characteristics of herbal paper soap. The experiment involved three extraction temperatures (60°C, 70°C, and 80°C) and two extraction durations (15 and 20 minutes), resulting in six treatment combinations. The findings indicate that an extraction temperature of 60°C for 15 minutes produced the best moisture content, and foam stability, while the optimal free alkali content was obtained at 80°C for 20 minutes. The highest antibacterial activity was observed at 70°C for 15 minutes. In the organoleptic evaluation, the best color scoring was achieved at 60°C for 20 minutes, aroma scoring at 80°C for 20 minutes, and thickness scoring at 60°C for 15 minutes. Further analysis revealed that extraction temperature and duration significantly influenced the physicochemical properties, including free alkali content, foam stability, and skin irritation, as well as organoleptic characteristics such as color, aroma, and thickness. However, these factors had no significant effect on moisture content and antibacterial activity. Overall, the paper soap met the quality standards outlined in SNI 06-3532-2016, except for free alkali content, which exceeded the maximum allowable limit of 0.1%, making it non-compliant with soap quality standards

References

P. Naomi, M. L. G. Anna, dan T. M. Yusuf, "Pembuatan sabun lunak dari minyak goreng bekas ditinjau dari kinetika reaksi kimia," Jurnal Teknik Kimia, vol. 19, no. 2, pp. 42-48, 2013.

F. Farid, M. S. Putri, dan R. Havizur, "Introduksi teknologi sabun cair antiseptik dari buah pedada (Sonneratia caseolaris) di Kelurahan Kampung Laut, Kuala Jambi, Tanjung Jabung Timur," Jurnal Karya Abadi Masyarakat, vol. 27, pp. 1-12, 2018.

I. P. Dewi dan W. Wela, "Formulasi dan evaluasi sabun kertas katekin sebagai antiseptik," PHARMACY: Jurnal Farmasi Indonesia (Pharmaceutical Journal of Indonesia), vol. 17, no. 2, pp. 514-523, 2021.

A. Widyasanti, A. M. L. Ginting, E. Asyifani, dan S. Nurjanah, "The production of paper soaps from coconut oil and Virgin Coconut Oil (VCO) with the addition of glycerine as plasticizer," in IOP Conference Series: Earth and Environmental Science, vol. 141, no. 1, p. 012037, Mar. 2018, IOP Publishing.

H. Izhar, Sumiati, dan P. Moeljadi, "Analisis sikap konsumen terhadap atribut sabun mandi (studi pada sabun mandi merek Lux dan Giv di Kota Malang)," WACANA, vol. 13, no. 4, pp. 615-630, 2010.

P. Setyopratomo, "Produksi asam lemak dari minyak kelapa sawit dengan proses hidrolisis," Jurnal Teknik Kimia, vol. 7, no. 1, pp. 26-31, 2013.

M. Inna, N. Atmania, dan S. Prismasari, "Potential use of Cinnamomum burmanii essential oil-based chewing gum as oral antibiofilm agent," Journal of Dentistry Indonesia, vol. 17, no. 3, pp. 80-86, 2010.

D. H. D. Nurani, E. Purwati, dan C. I. N. H. Safitri, "Formulasi dan uji mutu fisik sabun herbal padat ekstrak kulit batang kayu manis (Cinnamomum burmanni)," in Proc. 13th Mulawarman Pharmaceuticals Conference, e-ISSN: 2614-4778, 5-7 Apr. 2021.

K. S. Akabata, M. F. ZR, S. Kuntolaksono, dan S. Handayani, "Proses scale-up pembuatan sabun mandi sekali pakai dari palm cooking oil (PCO) dengan penambahan berbagai jenis parfum," Jurnal Ilmu Pengetahuan dan Teknologi (IPTEK), vol. 7, no. 1, 2023.

E. W. I. Hajar dan S. Mufidah, "Penurunan asam lemak bebas pada minyak goreng bekas menggunakan ampas tebu untuk pembuatan sabun," Jurnal Integrasi Proses, vol. 6, no. 1, pp. 22-27, 2016.

R. Muthmainnah, D. Rubiyanto, dan T. S. Julianto, "Formulasi sabun cair berbahan aktif minyak kemangi sebagai antibakteri dan pengujian terhadap Staphylococcus aureus," Indonesian Journal of Chemical Research, vol. 1, no. 2, pp. 44–50, 2016.

Verawaty, I. P. Dewi, dan W. Wela, “Formulasi dan evaluasi sabun kertas katekin sebagai antiseptik,” Jurnal Farmasi Indonesia, vol. 17, no. 2, 2020.

L. K. Tanno, R. Darlenski, S. Sánchez-Garcia, M. Bonini, A. Vereda, P. Kolkhir, D. Antolin-Amerigo, V. Dimov, C. Gallego-Corella, J. C. A. Becerra, dan A. Diaz, "International survey on skin patch test procedures, attitudes, and interpretation," World Allergy Organization Journal, vol. 9, no. 1, p. 8, 2016.

H. P. S. Makkar, G. Francis, dan K. Becker, “Bioactivity of phytochemicals in some lesser-known plants and their effects and potential applications in livestock and aquaculture production systems,” Animal, vol. 1, no. 9, pp. 1371–1391, 2007.

A. Widyasanti dan J. M. Rohani, “Pembuatan sabun padat transparan berbasis minyak zaitun dengan penambahan ekstrak teh putih,” Jurnal Penelitian Teh dan Kina, vol. 20, no. 1, pp. 13–29, 2017.

Badan Standardisasi Nasional Indonesia, Standar Mutu Sabun Mandi, SNI 06-3532-2016, Jakarta: Dewan Standar Nasional, 2016.

Dinastuti, A. A. Kiswandono, dan Fatimah, “Sabun susu sapi dengan penambahan kulit kayu manis sebagai antibakteri,” Analit, vol. 6, no. 1, pp. 66–73, 2021.

I. Sugiarti, “Antibacterial activity of liquid soap with cinnamon (Cinnamomum burmannii) extract,” Diploma thesis, Politeknik Harapan Bersama, Tegal, Indonesia, 2019.

F. Korompis, P. Yamlean, dan W. Lolo, “Formulasi dan uji efektivitas antibakteri sediaan sabun cair ekstrak etanol daun kersen (Muntingia calabura L.) terhadap bakteri Staphylococcus aureus,” Jurnal Pharmacon, vol. 3, no. 9, pp. 404–412, 2020.

P. K. R. Hadia, “Composition and evaluation of transparent solid soap made from VCO with lime juice (Citrus aurantifolia),” Undergraduate thesis, Universitas Andalas, Padang, Indonesia, 2006.

A. K. O. Sembiring, A. A. B. Putra, dan O. Ratnayani, “Utilization of cinnamon bark (Cinnamomum burmannii) extract as a natural inhibitor for the control of corrosion rate in iron metal,” Jurnal Ilmu Pendidikan Indonesia, vol. 11, no. 3, pp. 140–150, 2023.

D. Mulyani, H., dan L. Marliana, “Formulasi sabun padat dari biji kopi arabika (Coffea arabica L.) Kerinci,” JFSOT, vol. 2, no. 1, pp. 67–74, Jan. 2023.

D. Katrin dan N. Idiawati, “Uji aktivitas antibakteri dari ekstrak daun malek (Litsea graciae Vidal) terhadap bakteri Staphylococcus aureus dan Escherichia coli,” JKK, vol. 4, no. 1, pp. 7–12, 2015.

T. Fitriyani, “Effect of HPMC ratio as a gelling agent in scallion (Allium fistulosum L.) extract gel on the growth of Staphylococcus aureus,” Diploma thesis, Politeknik Harapan Bersama, Tegal, Indonesia, 2017.

M. B. Aqmarina, “Uji aktivitas antibakteri minyak kayu manis (Cinnamomum burmannii Nees ex Bl.) terhadap bakteri Staphylococcus aureus penyebab jerawat,” Prosiding Farmasi, vol. 2, no. 2, 2016.

A. G. Amrie, Ivan, S. Anam, dan Ramadhanil, “Uji efektivitas ekstrak daun dan akar Harrisonia perforata Merr. terhadap pertumbuhan bakteri Vibrio cholerae,” Journal of Natural Science, vol. 3, no. 3, pp. 331–340, 2015.

B. R. Noviano, C. Mambo, dan J. Wuisan, “Uji efek antibakteri kulit kayu manis (Cinnamomum burmannii) terhadap Escherichia coli dan Streptococcus pyogenes,” Jurnal e-Biomedik (eBm), vol. 4, no. 1, 2016.

I. Musfiroh, W. Indriyati, Muchtaridi, dan Y. Setiya, “Proximate analysis and determination of β-carotene content in tamarillo (Cyphomandra betacea Sendtn.) sheet jam using visible spectrophotometry,” Undergraduate thesis, Faculty of Pharmacy, Universitas Padjadjaran, Indonesia, 2007.

S. T. Soekarto, Penilaian Organoleptik untuk Industri Pangan dan Hasil Pertanian, Jakarta: Bharata Karya Aksara, 2002.

Z. S. Othman, M. Y. Maskat, dan N. H. Hassan, “Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract,” Sains Malaysiana, vol. 49, no. 5, pp. 995–1002, 2020.

M. K. Robinson dan M. A. Perkins, “A strategy for skin irritation testing,” American Journal of Contact Dermatitis, vol. 13, no. 1, pp. 21–29, Mar. 2002.

Downloads

Published

22-04-2025

Issue

Section

Articles